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working principle of study on optimal conditions of high purity poly ferric chloride

  • Isolation and purification of bacterial poly(3 ...

    2008-4-1 · Under optimal conditions – 30% (w/v) hypochlorite, 1:1 volume ratio of chloroform-to-aqueous phase, 4% (w/v) cells in dispersion, 30 °C, 90 min treatment – 91% P(3HB) could be recovered from R. eutropha with a high purity which exceeded 97% .

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  • Serum cholesterol measurement based on ethanol

    2. Color reagent The optimal concentration of ferric chloride hexahydrate was found to be 100 mg/ioo ml of ethyl acetate, that is 44.4 mg/ioo ml of final reaction mixture (Fig. 2). This result agrees with that obtained by Zak'. The effect of the anion associated with the ferric ion was tested by using ferric chloride, bromide and acetate.

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  • A comprehensive review on the synthesis and

    (1) Currently PEMFC is an expensive technology due to the high production cost of high purity hydrogen, and one research direction is to develop catalytic electrode materials which can function well in the presence of impurities; (2) the commonly used IEMs are not stable at high temperature PEMFC operation, so research is needed to develop low-cost membrane materials with excellent …

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  • High-poly-aluminum chloride sulfate coagulants and their ...

    2020-2-18 · High-poly-aluminum chloride sulfate (HPACS) coagulants with different [SO 4 2−]/[Al 3+] molar ratio (S) were prepared and proved to have high coagulation efficiency for the removal of humic acid and strong stability for storage and application.The results showed that the higher the SO 4 2− addition, the bigger the aluminum polymerization particles and the more the …

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  • A vacuum distillation process for separation of antimony ...

    2021-6-1 · The results indicate that the optimal temperature for separating Sb 2 S 3 and PbS are 923 K and 1173 K, respectively. Under optimal conditions, up to 98% of Sb 2 S 3 with a purity of 99.17% and up to 99.5% of PbS with a purity of 98.7% could be recovered.

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  • Pretreatment of landfill leachate in near-neutral pH ...

    2019-2-1 · Under the optimal experimental conditions, after 2 h treated by PS-ICME system, the concentrations of ferrous iron and ferric iron in effluent were 0.42 g L −1 and 3.78 g L −1, respectively. At neutral pH, the ferrous iron in the iron-carbon microelectrolysis system is easily converted into ferric iron, which combines with hydroxide to form Fe(OH) 2+ , Fe(OH) 2 + and …

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  • Review on feasible recycling pathways and technologies

    2015-10-1 · According to Powalla et al. , all existing thin-film PV technologies, especially the Cu(In,Ga)Se 2 (CIGS)-based technology, have a high cost reduction potential at high production volumes, projecting futuristic challenge to combine high production volumes with high throughput, sufficient yield and superior quality to achieve efficiencies of above 11% and a maximum of 12.7%.

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  • Applying Quality by Design Principles in the Development ...

    2020-3-3 · 131 I-labeled STI-571 was prepared with high radiochemical purity (>90%). Kumar et al. developed the procedure for radiolabeling of an anticancer drug tamoxifen with 99m Tc for tumor diagnosis and to evaluate the diagnostic effect of the radiolabeled compound in mice. Radiolabeling efficiency of tamoxifen with 99m Tc was found to be 97%. In vitro stability of the labeled complex …

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  • Concentrating and recycling of high-concentration

    2021-7-1 · 1. Introduction. The textile industry uses large volumes of fresh water .The shortage of healthy freshwater supply has become increasingly serious , and solving this problem is a key technical problem.. At present, a lot of valuable research has been carried out on the treatment of printing and dyeing wastewater .There exist many processes for the treatment and reuse of wastewater when the …

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  • Modern Chemical Industry - xdhg.com.cn

    2021-2-20 · In order to further improve the effects of microwave,molecular dynamics simulation method is utilized to study the effect of microwave field on simulated high pour point crude oil system.The intrinsic relationship between the properties of high pour point crude oil and its component molecules is analyzed,and the effect rules of microwave electric field on the properties of high …

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  • Isolation and purification of bacterial poly(3 ...

    2008-4-1 · Under optimal conditions – 30% (w/v) hypochlorite, 1:1 volume ratio of chloroform-to-aqueous phase, 4% (w/v) cells in dispersion, 30 °C, 90 min treatment – 91% P(3HB) could be recovered from R. eutropha with a high purity which exceeded 97% .

    Get Price
  • High-poly-aluminum chloride sulfate coagulants and their ...

    2020-2-18 · High-poly-aluminum chloride sulfate (HPACS) coagulants with different [SO 4 2−]/[Al 3+] molar ratio (S) were prepared and proved to have high coagulation efficiency for the removal of humic acid and strong stability for storage and application.The results showed that the higher the SO 4 2− addition, the bigger the aluminum polymerization particles and the more the …

    Get Price
  • High-Purity Salts - Sigma-Aldrich

    High-purity materials are crucial components for the research, development, and production of advanced technologies which require optimum properties, performance, and quality. We offer ultra-high purity salts with purity exceeding 99.998% (less than 10 parts per million trace metal impurities). Our ISO 9001 quality management system ensures ...

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  • Study of the electrodeposition conditions of metallic ...

    2010-6-1 · A high current efficiency and low specific energy consumption were favored at a pH of 7.5 with additive incorporation. Under the optimized conditions, a maximum current efficiency of 85.86% was attained with an electrolyte composition of 35 g/L Mn and 130 g/L (NH 4 ) 2 SO 4 at a temperature of 40 °C and a pH of 7.5 in the presence of additives ...

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  • Pretreatment of landfill leachate in near-neutral pH ...

    2019-2-1 · Under the optimal experimental conditions, after 2 h treated by PS-ICME system, the concentrations of ferrous iron and ferric iron in effluent were 0.42 g L −1 and 3.78 g L −1, respectively. At neutral pH, the ferrous iron in the iron-carbon microelectrolysis system is easily converted into ferric iron, which combines with hydroxide to form ...

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  • Overview of the recycling technology for copper-containing ...

    2017-11-1 · This process optimizes the working conditions; a cloth dust bag is used during the steps that produce a great deal of dust. Download : Download high-res image (250KB) Download : Download full-size image; Fig. 2. Schematic of the working principle for crushing technology .

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  • Lung cancer risk in workers exposed to poly(vinyl chloride ...

    Poly(vinyl chloride) (PVC), one of the most widely used plastic materials, is produced by polymerisation of vinyl chloride monomer (VCM). The VCM/PVC industry was the focus of a major occupational health crisis in the mid-1970s when an increased frequency of the rare liver angiosarcoma tumour was reported in workers exposed to over 10 000 ppm ...

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  • The Basics: RNA Isolation | Thermo Fisher Scientific - US

    2021-1-12 · where Δμ is the difference of the effective (net) mobilities between the enantiomers, μ 1 and μ 2 are the effective (net) mobilities of the first and the second migrating enantiomer, μ f the mobility of the non-complexed analyte and μ C1 and μ C2 the mobilities of the enantiomer-selector complexes. K 1 and K 2 are the complexation constants of enantiomer 1 and 2 with the chiral …

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  • Advances of capillary electrophoresis enantioseparations ...

    2021-1-13 · We present a simulation-based study for identifying promising cell structures, which integrate poly-Si on oxide junctions into industrial crystalline …

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  • Influence of the Supporting Electrolyte on the ...

    2016-7-12 · 95%. In any case, the results of this study allow selecting the electrosynthesis working conditions depending on the wanted application of the PEDOT modified electrode. Keywords: 3,4-ethylenedioxythiophene, electropolymerization, p-doping, n-doping, poly(3,4-ethylenedioxythiophene), nucleation and growth mechanism.

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  • Fabrication of ferric chloride doped polyaniline ...

    2016-6-18 · Nowadays, supercapacitors as a new class of energy storage and power supply devices are developed to meet the increasing demand for applications in powering vehicles and portable electronic devices because of their high power density, long cycle life, simple principle, and speedy dynamic of charge propagation [].Supercapacitors can store electrical charge by two …

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  • Preparation of FeS2/TiO2 nanocomposite films and study on

    2021-4-5 · Figure 6 shows the XPS spectra of FeS 2 /TiO 2 nanocomposite film prepared under hydrothermal reaction time of 12 h, ferric chloride concentration of 0.15 mmol/L and reaction temperature of 180 °C, among them, Fig. 6 a is the full spectrum scanning, and Fig. 6 b–e is the high resolution narrow spectrum scanning map of elements.

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  • Ultrasensitive Detection of Ferulic Acid Using Poly ...

    Furthermore, FTIR spectroscopy was also employed to investigate the reduction of the oxygen-containing groups in GO during the functionalized process [].As shown in Figure 2, after reduction of the GO (curve a) with hydrazine for 24 h, the FTIR peaks intensities in PDDA-G (curve b) corresponding to the oxygen functionalities, such as the C = O stretching vibration peak at 1724 …

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  • Synthesis of cross-linked poly(acrylic acid) nanogels in ...

    2019-11-6 · 1. Introduction. Micro- and nanogels are cross-linked polymers of micro–nanosize filled with a solvent. They can exist either in the swollen or the shrunken state depending on the environmental conditions [1–4].They exhibit very high surface areas, low viscosities and, compared with regular gels, can be injected into the body.

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  • Study on the Electrochemical Performance of Sacrificial ...

    2018-8-1 · The influence of sacrificial anode electrochemical properties interfered by direct stray current (DC) of 0 V, 1 V, 3 V, and 5 V, with different chloride ion concentration and temperature, was studied by open circuit potential (OCP), electrochemical impedance spectroscopy (EIS), and polarization curves. The specific performance was as follows: as the DC interference voltage …

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  • Advances and approaches for chemical recycling of plastic ...

    2020-8-11 · With poly-l-lysine, mismatched system DR2 shows nearly no FRET at similar conditions, with the highest FRET being around 7.5% at a ratio of …

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  • Optical and theoretical study of strand recognition by ...

    2011-8-16 · The phaZ Sex gene encoding poly(3-hydroxybutyrate) depolymerase from Streptomyces exfoliatus has been successfully cloned and expressed in Rhodococcus sp. T104 for the first time. Likewise, the recombinant enzyme was efficiently produced as an extracellular active form and purified to homogeneity by two hydrophobic chromatographic steps. MALDI-TOF …

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  • Extracellular production of Streptomyces exfoliatus poly(3 ...

    2013-4-4 · The electrospinning parameters can be adjusted to control final fiber characteristics. Some of the important parameters to consider are viscosity, molecular weight of the polymer, applied voltage, charge density, distance from needle to collector, humidity, etc. Controlling these parameters is a crucial step to obtaining electrospun fibers with properties that meet specific …

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  • Development of Polymer-based Chemical Sensor to Study the ...

    2020-2-17 · Under optimal conditions, the polymer based electrochemical sensor PVA/GCE displayed a linear range to GA in the concentration of 1.6 × 10-6-to 4.9 × 10 5 mol L 1 with a detection limit of 4.95 x 10-7 mol L 1. Keywords: Electrochemical modified electrode, freeze-thaw cycle, gallic acid, PVA hydrogel, square wave voltammetry 1. INTRODUCTION

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  • Chiral Capillary Electrokinetic Chromatography: Principle ...

    2021-5-1 · Preconcentration by solid phase extraction, fused silica capillary of 75 µm i.d. and 365 µm o.d., separation voltage from 10 to 12 kV, BGE of 75 mM phosphate buffer pH 3.0 and 0.9% poly (diallyldimethylammonium chloride), hydroxypropyl-γ-CD as a CS. UV at 254 nm: 2.1 to 6.3 nM-

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  • Frontiers | Facial Fabrication and Characterization of ...

    2020-11-3 · In this study, a novel chloride ion (Cl−) sensor based on Ag wire coated with an AgCl layer was fabricated using a gel-type internal electrolyte and a diatomite ceramic membrane, which played an important role in preventing electrolyte leakage from the ion-selective electrode. The sensing performance, including reversibility, response, recovery time, low detection limit, and the …

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  • Performance Analysis of Thermoacoustic Refrigerator of 10 ...

    2015-12-16 · Experimental study and computer simulation of the high conversion reaction at 130 °C”, Polymer 22(7), 928–933 (1981). CAS Article Google …

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  • A New Route for High-Purity Organic Materials: High ...

    2016-1-11 · Following the parametric study, a number of optimal stable jetting conditions were found that could be used for high-resolution pattern printing. As mentioned previously, 245 °C was chosen for printing 2D patterns such as squares and spiral shapes (figures 9(a) and ). Both of these patterns could be printed with high efficiency.

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  • 3D printing of high-resolution PLA-based structures by ...

    2021-2-26 · Chloride solution (100 mg L –1) was used to study the effect of volume of chloride solution on the length of the white-colored band by keeping the volume and concentration of silver nitrate constant at 7.5 μL and 0.1 mol L –1, respectively. Figure 4 shows that the length of the white-colored band increased with volume in a range of 15–45 ...

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  • Application of Differential Scanning Calorimetry to the ...

    2014-7-6 · In the present study, a novel enzyme-based grafting of poly(3-hydroxybutyrate) [P(3HB)] onto the ethyl cellulose (EC) as a backbone polymer was developed under a mild and ecofriendly environment and laccase was used as a grafting tool. The resulting composites were characterised using various instrumental and imaging techniques. The high intensity of the 3,358 …

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  • Indicator-Free Argentometric Titration for Distance-Based ...

    The working principle of a photodiode is, when a photon of ample energy strikes the diode, it makes a couple of an electron-hole. This mechanism is also called the inner photoelectric effect. If the absorption arises in the depletion region junction, then the carriers are removed from the junction by the inbuilt electric field of the depletion ...

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  • Cellulose, nanocellulose, and antimicrobial materials for ...

    2021-7-10 · High-purity pulp has weak bonding and low strength properties, but it provides high bulk and permeability, two important properties for filter media that are directly affected by the level of purity of the wood pulp (Hutten 2016). Chemical pulping includes the alkaline kraft, the acidic sulfite, and the organosolv processes.

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  • Journal of Physics: Conference Series, Volume 1825, 2021 ...

    2021-3-12 · International Conference on Physics and Its Applications (ICOPIA) is a biannual conference, started in 2001. This year of 2020, ICOPIA is the tenth one. This conference is mainly supported by Department of Physics, Universitas Sebelas Maret, Indonesia. ICOPIA is a forum for presenting and discussing current research in physics and its applications.

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  • 2.3. Algal production

    2015-11-17 · In the experiment, electrophoresis gel is divided into two layers: the upper one is a macroporous gel with low concentration, called stacking gel, buffer for the formulation of this layer is Tris-HCl, pH6.7; the lower one is hole glue with high concentrations, called separating gel or electrophoresis gel , and the buffer for this is Tris-HCl ...

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  • Principle and Protocol of Sodium Dodecyl Sulphate ...

    An ECL analyzer was established in this study, and it was shown that this analyzer was stable and highly sensitive, with a detection range of 0.4 pmol to 4 nmol Ru(bpy) 3 Cl 2 ·6H 2 O under optimal reaction conditions of 1.0 V, 1.0 mA, 1.5 mol·L −1 TPrA, and pH 7.4. The optimal amount of magnetic beads for separation of labeled NPA probes ...

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  • Detection of Prorocentrum minimum (Pavillard) Schiller ...

    2020-3-31 · In principle, the solubility of PVAs strongly depends on their hydrolysis degree, molecular weight, and crystallinity . According to the literature, both PVAs with a high (>95%) and low (87 to 89%) degree of hydrolysis are soluble in water at the conditions that we used for the preparation of the pregel solution (i.e., mixing at 98 °C and then ...

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  • Twin-chain polymer hydrogels based on poly(vinyl alcohol ...

    The European Commission asked the European Food Safety Authority (EFSA) to prepare a statement on a framework for conducting the environmental exposure and risk assessment for transition metals and their compounds (e.g. salts) from the chemical periodic table of element groups 7–11 of period 4 (iron, cobalt, nickel and copper) when used as active substances in plant …

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  • Introduction, Principle, Instrumentation and Applications ...

    2017-4-21 · Metal–organic framework (MOF) materials are well known for various application fields, such as engineering, and medical sciences. Here, the synthesis, and synthesis-optimisation of a novel oxalate-phosphate-amine MOF (OPA-MOF) for innovative agricultural applications is described, with urea as a structure-directing agent in a hydrothermal synthesis. Product …

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  • Determination of the Labile Iron Pool of Human

    2007-9-17 · Subsequent to the measurement of the initial fluorescence (λ ex = 425± 22.5 nm, λ em = 450–490 nm) of lymphocytes that had been loaded with 30 μM CP655 (for 10 min, in HBSS, 37 °C), either the iron complex (ferric chloride:8-hydroxyquinoline = 15 μM : 30 μM) or the strong iron chelator, CP94 (1 mM), was added to the supernatant and the ...

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  • Dual-lifetime referencing (DLR): a powerful method for on ...

    2021-4-14 · 科学研究-欢迎来到亚稳材料制备技术与科学国家重点实验室. 当前位置: 首页 >> 科学研究. 论文名称. 刊物名称. 论文所在期刊的卷、期、页. 论文作者. 影响因子. Nanotwinned diamond with unprecedented hardness and stability. NATURE.

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  • Annelise E. Barron's Profile | Stanford Profiles

    2012-3-28 · Determination of internal pH in enzyme immobilizates: Choice of materials, set-up of the analytical system, and sensor calibration. A DLR system was established using two luminophores of which one, fluorescein, displays pH-sensitive fluorescence behavior and the other, Ru(II) tris(4,7-diphenyl-1,10-phenantroline), abbreviated Ru(dpp), does not respond to pH and …

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  • Optimization and economic evaluation of modified ...

    Annelise E. Barron is the W.M. Keck Associate Professor of Bioengineering at Stanford University. The broad theme of the Barron lab is the study and biomimicry of natural host defense peptides (antimicrobial peptides). We study the molecular biophysics and mechanisms of LL-37—a centrally important human host defense peptide—and its ...

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  • Poly(-β-hydroxybutyrate) (PHB) depolymerase PHAZ Pen

    2018-10-17 · Chemicals. Poly-aluminum chloride (Al 2 (OH) n Cl 6−n.YH 2 O, Al 2 O 3 = 30%wt, basicity = 65% and pH = 3) was used as a coagulant and anionic (A 300), cationic (C 270) and nonionic polymers, as the coagulant aids were provided from AquaTech Company, Switzerland.. Preparation of solution. In order to prepare a 10 percent clear solution for coagulant, 10 g of PAC …

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  • Philosophy of Chemistry (Stanford Encyclopedia of

    2015-3-24 · Very few studies have been dedicated to R-hydroxyacids (R-HA) production using extracellular polyhydroxyalkanoate depolymerases (ePhaZs). Penicillium expansum produced maximum extracellular polyhydroxybutyrate depolymerase (~6 U/mL) by 72 h when grown in mineral salt medium containing 0.2 % w/v PHB, pH 5.0, at 30 °C and 200 rpm shaking conditions. …

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  • Polyesters: Characteristics and Applications

    The method is economical and the product is of high purity. The technique is used for preapring polyvinyl chloride (PVC) polystyrene (PS) polymethymethacrylate (PMMA). Solution polymerization:- the monomer and catalyst (free radical, cationic and anionic) are dissolved in a suitable inert solvent.

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  • Journal of the Electrochemical Society, Volume 148,

    High-purity aluminum foils were examined using positron annihilation spectroscopy (PAS) after dissolution for various times in 1 M NaOH at room temperature. Measurements of the S and W shape parameters of the annihilation photopeak at 511 keV show the presence of voids of at least nanometer dimension located at the metal-oxide film interface.

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  • The Biomedical Use of Silk: Past, Present, Future ...

    In a comprehensive in vivo study of small diameter electrospun silk graft performance, Filipe et al. have demonstrated the production and performance of electrospun acellular silk fibroin grafts generated under aqueous conditions in the absence of chemical cross-linkers (Figure 7). The electrospun silk fibroin grafts were significantly more ...

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  • PERFORMANCE ASSESMENT OF A POLYMER ELECTROLYTE

    2021-4-14 · 科学研究-欢迎来到亚稳材料制备技术与科学国家重点实验室. 当前位置: 首页 >> 科学研究. 论文名称. 刊物名称. 论文所在期刊的卷、期、页. 论文作者. 影响因子. Nanotwinned diamond with unprecedented hardness and stability. NATURE.

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  • Journal of the Electrochemical Society, Volume 148,

    2018-4-23 · novel alkaline anion-exchange membrane based on Chitosan (CS) and Poly(vinyl) alcohol (PVA) in a 50:50 composition ratio doped with a 5 wt.% of poly (4-vinylpyridine) organic ionomer cross-linked, methyl chloride quaternary salt resin (4VP) was assessed as solid polymer electrolyte. The influence of 4VP anionic ionomer loading of 7, 12 and 20 wt.%

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  • Phosphorus Removal and Recovery from Digestate after ...

    High-purity aluminum foils were examined using positron annihilation spectroscopy (PAS) after dissolution for various times in 1 M NaOH at room temperature. Measurements of the S and W shape parameters of the annihilation photopeak at 511 keV show the presence of voids of at least nanometer dimension located at the metal-oxide film interface.

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  • High elasticity, chemically recyclable, thermoplastics ...

    a ROP reaction conditions: [1] : [CHD] = 1 : 4, 100 °C, toluene. b ROCOP reaction conditions: [2] : [PPN-PDL-PPN] : [LO] = 1 : 0.25 : 125, 20 bar CO 2, 45 °C. c M n and Đ measured by SEC (THF eluent, calibrated using polystyrene standards). d Weight % of PLC block, determined from the 1 H NMR spectra, by analysis of the integrals of PLC and ...

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  • Bacteriology Culture Guide | ATCC

    When working with anaerobic cultures, it is important to avoid unnecessary exposure to oxygen. Anaerobic conditions may be obtained for either transfer or incubation by the methods listed below. Unless specifically mentioned, the standard anaerobic gas mixture is …

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  • Selective ion sensing with high resolution large area ...

    2020-6-26 · All-solid-state sodium-selective electrode based on a calixarene ionophore in a poly (vinyl chloride) membrane with a polypyrrole solid contact. Anal. Chem. 64 , 2496–2501 (1992).

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  • Beaker 250 mL Wash bottle Initial Conditions Obtain 10 mL ...

    2019-10-8 · Industrial Production. What do paper, soap, and (some) clothing have in common? We need to use sodium hydroxide (NaOH) to make them! As of 2004, we produce 60 million metric tons per year worldwide!

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  • Full Awards: Teen Scientists and Engineers Win $5 Million

    2021-5-21 · Washington, D.C.—Society for Science and Regeneron announced Grand Awards of the Regeneron ISEF 2021. Student winners are in ninth through twelfth grades who earned the right to compete at the Regeneron ISEF 2021 by winning a top prize at a local, regional, state or national science fair. Grand Awards are presented in each of the […]

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  • Professor Behdad Moghtaderi Staff Profile The ...

    2016-10-28 · Aqueous two-phase system (ATPS) is a liquid-liquid fractionation technique and has gained an interest because of great potential for the extraction, separation, purification and enrichment of proteins, membranes, viruses, enzymes, nucleic acids and other biomolecules both in industry and academia. Although, the partition behavior involved in the method is complex and …

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  • Aqueous two-phase system (ATPS): an overview and

    2021-4-29 · This project will aim to study the flow (flow patterns and overall homogeneity) and power characteristics of high shear mixers. The study will build on the previous work of the supervisor and make use of bench scale high shear process devices- a selection of rotor-stator designs and an ultrasonicator- in both batch and re-circulation mode.

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  • Indicative projects | Chemical Engineering |

    2013-10-22 · Authors of one study encourage clinicians to incorporate HIIT, performed three times a week for at least 12 weeks, into exercise programs for obese patients. 19 Another recent review looking at HIIT in patients with coronary heart disease found that the optimal protocol involved short interval duration (15 seconds) and maintaining close work ...

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  • CO2 separation membranes with high permeability and

    2017-8-1 · The high thermal stability is due to the fact that aromatic ester groups cannot be broken by β-elimination processes because of the absence of hydrogen in the β-position . This study put in evidence the validity of the dendritic characteristics in the improvement of epoxy thermosets.

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  • Influence of charged groups on the cross-linking ...

    The known understanding can in principle be used when working with proteins [MYE01]. Kinetics, meaning nucleation, crystal growth and dissolution, and thermodynamics, ... chloride, which is a pure and one component crystal, basically depends on the ... poly-ionic character of the proteins and the solutions they exist in are of great importance.

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  • Exercise prescription and basic principles of therapeutic ...

    Working conditions of the system can be easily adjusted for different sample concentration ranges. The limit of detection for the determination of acetylcholine was found to be 8x10(-5) M. The method described could be advantageously used for indirect determination of …

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